1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

Base Information

Chemical Name:1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid
CAS No.:266338-76-5
Molecular Formula:C₂₁H₂₈N₂O₅
Molecular Weight:388.464
Hs Code.:

Synonyms:1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

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Chemical Property of 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

Chemical Property:

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Technology Process of 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

There total 5 articles about 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 266338-72-1
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

: 266338-76-5
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 26h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 529-64-6,28845-94-5
Tropic acid

: 266338-76-5
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-76-5
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}cyclopentanecarboxilic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

4: 100 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition / 4: Hydrolysis;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1