1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

Base Information

Chemical Name:1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide
CAS No.:266338-72-1
Molecular Formula:C₂₃H₃₃N₃O₄
Molecular Weight:415.533
Hs Code.:

Synonyms:1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

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Chemical Property of 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

Chemical Property:

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Technology Process of 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

There total 4 articles about 1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-69-6
1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]-cyclopentanecarboxilic acid

: 266338-72-1
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: In acetonitrile; at 20 ℃; for 25h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 529-64-6,28845-94-5
Tropic acid

: 266338-72-1
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-72-1
1-{1-[(3-hydroxy-1-oxo-2-phenylpropyl)amino]cyclopentanecarboxamido}-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / acetonitrile / 48 h / 20 °C

2: 99 percent / aq. HCl / tetrahydrofuran / 24 h / 20 °C

3: 90 percent / acetonitrile / 25 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1