((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

Base Information

Chemical Name:((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)
CAS No.:219638-18-3
Molecular Formula:C₂₀H₂₄N₂O₅
Molecular Weight:372.421
Hs Code.:

Synonyms:((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

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Chemical Property of ((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

Chemical Property:

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Technology Process of ((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

There total 3 articles about ((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 219638-17-2
2-amino-3-(5-benzyloxy-pyridin-2-yl)-propionic acid

: 24424-99-5
di-tert-butyl dicarbonate

: 219638-18-3
((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

Guidance literature:: With sodium carbonate; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2005.06.048

Reference yield:

: 219638-16-1
2-acetylamino-2-(5-benzyloxy-pyridin-2-ylmethyl)-malonic acid diethyl ester

: 219638-18-3
((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq. H₂SO₄

2: 99 percent / aq. Na₂CO₃ / tetrahydrofuran

With sulfuric acid; sodium carbonate; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2005.06.048

Reference yield:

: 127590-90-3
3-(benzyloxy)-6-(chloromethyl)pyridine

: 219638-18-3
((±)-3-(5-(benzyloxy)pyridine-2-yl)-2-(tert-butoxycarbonylamino)propanoic acid)

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / t-BuOK / dimethylformamide

2: 90 percent / aq. H₂SO₄

3: 99 percent / aq. Na₂CO₃ / tetrahydrofuran

With sulfuric acid; potassium tert-butylate; sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.06.048