2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Base Information

Chemical Name:2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane
CAS No.:126993-25-7
Molecular Formula:C₁₃H₁₇BrO₂
Molecular Weight:285.181
Hs Code.:
DSSTox Substance ID:DTXSID201231440

Synonyms:2-(bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane;DTXSID201231440;126993-25-7

Suppliers and Price of 2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:284.04119
Heavy Atom Count:16
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(COC(OC1)(CBr)C2=CC=CC=C2)C

Technology Process of 2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

There total 3 articles about 2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 65849-85-6
3,3,9,9-Tetramethyl-1,5,7,11-tetraoxaspiro<5.5>undecan

: 70-11-1
α-bromoacetophenone

: 3592-12-9
5,5-dimethyl-1,3-dioxan-2-one

: 126993-25-7
2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 0.75h; chemoselective reaction;
DOI:10.3184/030823408X382126

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 70-11-1
α-bromoacetophenone

: 126993-25-7
2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Reflux;

Reference yield:

: 98-86-2
acetophenone

: 126993-25-7
2-(Bromomethyl)-5,5-dimethyl-2-phenyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide

2: toluene-4-sulfonic acid / toluene

With N-Bromosuccinimide; toluene-4-sulfonic acid; In toluene;
DOI:10.1021/acs.jafc.2c00541