N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Base Information

Chemical Name:N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide
CAS No.:477908-30-8
Molecular Formula:C₁₉H₂₅N₃O₅S
Molecular Weight:407.491
Hs Code.:

<i>N</i>-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Synonyms:N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Suppliers and Price of N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

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Technology Process of N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

There total 11 articles about N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3099-31-8
nicotinyl chloride

: 477908-30-8
N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide

2: MaOMe; HONH₂*HCl / methanol / 20 °C

3: K₂CO₃ / dimethylformamide

With hydroxylamine hydrochloride; potassium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 333-27-7
methyl trifluoromethanesulfonate

: 161314-70-1
N-hydroxy-2(R)-[[(4-methoxyphenyl)sulfonyl](3-picolyl)amino]-3-methylbutanamide

: 477908-30-8
N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; In methanol; acetonitrile; at 20 ℃;
DOI:10.1002/jlcr.570

Reference yield:

: 640-68-6,25609-85-2,7004-03-7,921-10-8
D-Val-OH

: 477908-30-8
N-methoxy-2-[(4-methoxy-benzenesulfonyl)-pyridin-3-ylmethyl-amino]-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / SOCl₂ / 20 °C

2: 83 percent / iPr₂NEt / acetonitrile / 48 h / 20 °C

3: 93 percent / K₂CO₃ / dimethylformamide / 20 °C

4: 46 percent / hydroxylamine hydrochloride; sodium methoxide / methanol / 48 h / 20 °C

5: tetrabutylammonium hydroxide / acetonitrile; methanol / 20 °C

With thionyl chloride; hydroxylamine hydrochloride; tetra(n-butyl)ammonium hydroxide; sodium methylate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/jlcr.570