C₂₆H₄₁F₂NO₂SSi₂

Base Information

• Chemical Name: C₂₆H₄₁F₂NO₂SSi₂
• CAS No.: 1628946-76-8
• Molecular Formula: C₂₆H₄₁F₂NO₂SSi₂
• Molecular Weight: 525.851
• Mol file: 1628946-76-8.mol

Synonyms:C₂₆H₄₁F₂NO₂SSi₂

Chemical Property of C₂₆H₄₁F₂NO₂SSi₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₁F₂NO₂SSi₂

There total 4 articles about C₂₆H₄₁F₂NO₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

chloro-trimethyl-silane (75-77-4) + C23H33F2NO2SSi (1628946-75-7) → C26H41F2NO2SSi2 (1628946-76-8)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1002/chem.201402506

Reference yield:

(difluoromethyl)(imino)(phenyl)-λ6-sulfanone (1333375-53-3) → C26H41F2NO2SSi2 (1628946-76-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / tetrahydrofuran / 0.05 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With 1H-imidazole; boron trifluoride diethyl etherate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/chem.201402506

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → C26H41F2NO2SSi2 (1628946-76-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.08 h / 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / tetrahydrofuran / 0.05 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With 1H-imidazole; boron trifluoride diethyl etherate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/chem.201402506

upstream raw materials:

(difluoromethyl)(imino)(phenyl)-λ⁶-sulfanone

chloro-trimethyl-silane

C₂₃H₃₃F₂NO₂SSi

tert-butyldimethylsilyl chloride

Downstream raw materials:

1,1-Difluoro-5-phenyl-pent-1-en-3-ol