((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

Base Information

Chemical Name:((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate
CAS No.:915772-16-6
Molecular Formula:C₁₈H₂₂O₇
Molecular Weight:350.368
Hs Code.:

Synonyms:((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

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Chemical Property of ((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

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Technology Process of ((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

There total 5 articles about ((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1336911-25-1
3,4,6-tri-O-ethoxycarbonyl-D-glucal

: 100-63-0
phenylhydrazine

: 915772-16-6
((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

Guidance literature:: With 1,10-Phenanthroline; oxygen; palladium diacetate; In acetic acid; at 65 ℃; for 6h;
DOI:10.1021/jo401032r

Reference yield:

: 541-41-3
chloroformic acid ethyl ester

: 130405-48-0
(2R,3S,6S)-2-(hydroxymethyl)-6-phenyl-3,6-dihydro-2H-pyran-3-ol

: 915772-16-6
((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol0618252

Reference yield:

: 125412-60-4
C-[4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl]benzene

: 915772-16-6
((2R,3S,6S)-6-phenyl-2-((ethoxycarbonyloxy)methyl)-3,6-dihydro-2H-pyran-3-yl)methyl ethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: macroporous carbonate resin / methanol / 5 h

2: 136 mg / pyridine / CH₂Cl₂ / 12 h / 20 °C

With pyridine; macroporous carbonate resin; In methanol; dichloromethane;
DOI:10.1021/ol0618252