{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

Base Information

Chemical Name:{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester
CAS No.:943776-93-0
Molecular Formula:C₂₂H₁₅BrCl₃N₃O₆
Molecular Weight:603.641
Hs Code.:

Synonyms:{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

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Chemical Property of {4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

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Technology Process of {4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

There total 4 articles about {4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 943772-71-2
4-(4-amino-phenoxy)-N-(4-bromo-phenyl)-3-nitro-benzamide

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 943776-93-0
{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

Guidance literature:: 4-(4-amino-phenoxy)-N-(4-bromo-phenyl)-3-nitro-benzamide; 2,2,2-Trichloroethyl chloroformate; With pyridine; In dichloromethane; for 4h;

With hydrogenchloride; In water; for 0.5h; pH=5;

Reference yield:

: 329941-08-4
N-(4-bromo-phenyl)-4-chloro-3-nitro-benzamide

: 943776-93-0
{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.42 h / 100 °C

1.2: pH 6

2.1: pyridine / dichloromethane / 4 h

2.2: 0.5 h / pH 5

With pyridine; potassium hydroxide; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 106-40-1
4-bromo-aniline

: 943776-93-0
{4-[4-(4-bromo-phenylcarbamoyl)-2-nitro-phenoxy]-phenyl}-carbamic acid 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 17 h / 20 °C

2.1: potassium hydroxide / dimethyl sulfoxide / 0.42 h / 100 °C

2.2: pH 6

3.1: pyridine / dichloromethane / 4 h

3.2: 0.5 h / pH 5

With pyridine; potassium hydroxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; dimethyl sulfoxide;