(1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde

Base Information

• Chemical Name: (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde
• CAS No.: 78796-73-3
• Molecular Formula: C₁₃H₁₀O₅
• Molecular Weight: 246.219

Synonyms:(1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde

Chemical Property of (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde

Chemical Property:

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SDS file from LookChem

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Technology Process of (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde

There total 2 articles about (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-12-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.7%

Oxytetracycline (79-57-2) → tertamethylammonium iodide (75-58-1) + 2,3,6-trihydroxybenzamide (101495-28-7) + (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-12-carbaldehyde (78796-73-3) + terramycin hydroiodide (78796-72-2)

Guidance literature:

With methyl iodide; In acetone; for 336h; Ambient temperature;

DOI:10.1016/S0040-4020(01)92015-0

Reference yield: 12.7%

Oxytetracycline (79-57-2) + methyl iodide (74-88-4) → tertamethylammonium iodide (75-58-1) + 2,3,6-trihydroxybenzamide (101495-28-7) + (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-12-carbaldehyde (78796-73-3) + terramycin hydroiodide (78796-72-2)

Guidance literature:

In acetone; for 336h; Ambient temperature;

DOI:10.1016/S0040-4020(01)92015-0

Reference yield:

methanol (67-56-1) + (1S,9R,12S)-6-Hydroxy-1-methyl-8,10-dioxo-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-12-carbaldehyde (78796-73-3) → (1S,9R,12S)-12-Dimethoxymethyl-6-hydroxy-1-methyl-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-triene-8,10-dione (78796-75-5)

Guidance literature:

With hydrogenchloride; for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)92015-0

upstream raw materials:

Oxytetracycline

methyl iodide

Downstream raw materials:

(1S,9R,12S)-12-Dimethoxymethyl-6-hydroxy-1-methyl-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-triene-8,10-dione

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