(5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one

Base Information

• Chemical Name: (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one
• CAS No.: 612817-40-0
• Molecular Formula: C₁₉H₂₀N₂O₄
• Molecular Weight: 340.379

Synonyms:(5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one

Chemical Property of (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one

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Technology Process of (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one

There total 1 articles about (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Phenoxyacetyl chloride (701-99-5) + (5S,6R)-4,5-dimethyl-6-phenyl-3,4,5,6-tetrahydro-2H-1,3,4-oxadiazin-2-one (397332-61-5,16638-85-0) → (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one (612817-40-0)

Guidance literature:

With lithium hydride; In 1,2-dichloro-ethane; Heating;

DOI:10.1016/j.tetasy.2003.07.020

Reference yield: 88.0%

4-chlorobenzaldehyde (104-88-1) + (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one (612817-40-0) → (2'S,3'R,5S,6R)-3,4,5,6-tetrahydro-3-[3-(4-chlorophenyl)-3-hydroxy-2-phenoxypropionyl]-4,5-dimethyl-6-phenyl-2H-1,3,4-oxadiazin-2-one

Guidance literature:

With titanium tetrachloride; triethylamine; In tetrahydrofuran; at -78 - 25 ℃; for 4h;

DOI:10.1016/j.tetasy.2003.07.020

Reference yield: 79.0%

4-methoxy-benzaldehyde (123-11-5) + (5S,6R)-3,4,5,6-tetrahydro-4,5-dimethyl-3-(2-phenoxyacetyl)-6-phenyl-2H-1,3,4-oxadiazin-2-one (612817-40-0) → (2'S,3'R,5S,6R)-3,4,5,6-tetrahydro-3-[3-hydroxy-3-(4-methoxyphenyl)-2-phenoxypropionyl]-4,5-dimethyl-6-phenyl-2H-1,3,4-oxadiazin-2-one

Guidance literature:

With titanium tetrachloride; triethylamine; In tetrahydrofuran; at -78 - 25 ℃; for 4h;

DOI:10.1016/j.tetasy.2003.07.020

upstream raw materials:

Phenoxyacetyl chloride

(5S,6R)-4,5-dimethyl-6-phenyl-3,4,5,6-tetrahydro-2H-1,3,4-oxadiazin-2-one

Downstream raw materials:

(5S,6R)-4,5-dimethyl-6-phenyl-3,4,5,6-tetrahydro-2H-1,3,4-oxadiazin-2-one

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