ethyl 3-(benzyloxy)cyclobutanecarboxylate

Base Information

• Chemical Name: ethyl 3-(benzyloxy)cyclobutanecarboxylate
• CAS No.: 106596-81-0
• Molecular Formula: C14H18 O3
• Molecular Weight: 234.29
• Hs Code.: 2918990090
• Mol file: 106596-81-0.mol

Synonyms:Cyclobutanecarboxylicacid, 3-(benzyloxy)-, ethyl ester (6CI); Ethyl3-(benzyloxy)cyclobutanecarboxylate

Chemical Property of ethyl 3-(benzyloxy)cyclobutanecarboxylate

Chemical Property:

• Boiling Point: 175 °C(Press: 10 Torr)
• PSA: 35.53000
• Density: 1.0632 g/cm3(Temp: 25 °C)
• LogP: 2.54490

Purity/Quality:

97% ^*data from raw suppliers

Ethyl 3-(benzyloxy)cyclobutanecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 3-(benzyloxy)cyclobutanecarboxylate

There total 5 articles about ethyl 3-(benzyloxy)cyclobutanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

epi-bromohydrin, benzyl bromide + diethyl malonate (105-53-3) → 3-benzyloxy-cyclobutanecarboxylic acid ethyl ester (106596-81-0)

Guidance literature:

In hexane; ethyl acetate;

Reference yield:

(2-bromo-1-bromomethylethoxymethyl)benzene (35995-55-2) → 3-benzyloxy-cyclobutanecarboxylic acid ethyl ester (106596-81-0)

Guidance literature:

Multi-step reaction with 3 steps

1: Na

2: (i) (saponification), (ii) (decarboxylation)

With sodium;

DOI:10.1021/jo01269a056

Reference yield:

benzyl bromide (100-39-0) → 3-benzyloxy-cyclobutanecarboxylic acid ethyl ester (106596-81-0)

Guidance literature:

Multi-step reaction with 4 steps

1: HgCl₂

2: Na

3: (i) (saponification), (ii) (decarboxylation)

With sodium; mercury dichloride;

DOI:10.1021/jo01269a056

upstream raw materials:

ethanol

3-(benzyloxy)cyclobutane-1-carboxylic acid

diisoamyl 3-benzyloxycyclobutane-1,1-dicarboxylate

(2-bromo-1-bromomethylethoxymethyl)benzene

Downstream raw materials:

ethyl 3-oxocyclobutanecarboxylate

cis-3-phenylcyclobutanecarboxylic acid

(1s,3s)-3-(4-fluorophenyl)cyclobutanecarboxylic acid

cis-3-(m-Tolyl)-cyclobutancarbonsaeure

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