(alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

Base Information

Chemical Name:(alpha-ethylphenacyl)-p-methoxyphenyllead diacetate
CAS No.:84840-86-8
Molecular Formula:C₂₁H₂₄O₆Pb
Molecular Weight:579.618
Hs Code.:

Synonyms:(alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

Suppliers and Price of (alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

There total 1 articles about (alpha-ethylphenacyl)-p-methoxyphenyllead diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18649-43-9
4-methoxyphenyllead(IV) triacetate

: 84839-88-3
trimethyl{(1-phenylbut-1-en-1-yl)oxy}silane

: 84840-86-8
(alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

Guidance literature:: With BF₃-Et₂O; In chloroform; the Pb-compd. and the silyl ether are dissolved in dry CHCl3 and then BF3-Et2O is added, the mixt. is stirred at room temp. for 2 h; the mixt. is diluted with CHCl3, then shaken with H2O and the CHCl3 layer is filtered, the solvent is evaporated and the product is triturated with pentane and dried, elem. anal.;
DOI:10.1039/P19930001677

Reference yield:

: 84840-86-8
(alpha-ethylphenacyl)-p-methoxyphenyllead diacetate

: 35258-39-0
2-(p-methoxyphenyl)-1-phenylbutan-1-one

: 301-04-2
lead acetate

: 100-66-3
methoxybenzene

: 495-40-9
propiophenone

: bis-(p-methoxyphenyllead) diacetate

Guidance literature:: In chloroform-d1; the Pb-compd. is stirred in dry CDCl3 at 60°C for 3 days; the ppt. is allowed to settle and analysis of the supernatant soln. by 1H.NMR, analysis by GLC, the crude product obtained on evapn. of the solvent is fractionated by HPLC in ethyl acetate-light petroleum to yield the butanone-compd.;
DOI:10.1039/P19930001677