Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester

Base Information

• Chemical Name: Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester
• CAS No.: 70508-49-5
• Molecular Formula: C₁₁H₇ClF₉O₃P
• Molecular Weight: 424.587
• Mol file: 70508-49-5.mol

Synonyms:Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester

Chemical Property of Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester

There total 1 articles about Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.9%

2,2,3,3,4,4,5,5,5-nonafluoropentanol (355-28-2) + O-phenyl phosphorodichloridate (770-12-7) → Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester (70508-49-5) + Phosphoric acid bis-(2,2,3,3,4,4,5,5,5-nonafluoro-pentyl) ester phenyl ester (70508-50-8)

Guidance literature:

With lithium chloride; for 0.7h; bath temperature 185 - 190 deg C;

DOI:10.1007/BF00958399

Reference yield: 88.0%

2,2,2-trifluoro-1-(4-methylphenyl)ethanol (446-65-1) + Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester (70508-49-5) → Phosphoric acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester 2,2,2-trifluoro-1-p-tolyl-ethyl ester

Guidance literature:

With magnesium; at 200 ℃; for 0.75h;

Reference yield: 83.0%

1-phenyl-2,2,2-trifluoromethylethanol (340-04-5,340-05-6) + Phosphorochloridic acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester (70508-49-5) → Phosphoric acid 2,2,3,3,4,4,5,5,5-nonafluoro-pentyl ester phenyl ester 2,2,2-trifluoro-1-phenyl-ethyl ester

Guidance literature:

With magnesium; at 200 ℃; for 0.75h;

upstream raw materials:

2,2,3,3,4,4,5,5,5-nonafluoropentanol

O-phenyl phosphorodichloridate