2-methyl-4-pyridinol nitrate

Base Information

Chemical Name:2-methyl-4-pyridinol nitrate
CAS No.:18614-65-8
Molecular Formula:C₆H₇NO*HNO₃
Molecular Weight:172.141
Hs Code.:

Synonyms:2-methyl-4-pyridinol nitrate

Suppliers and Price of 2-methyl-4-pyridinol nitrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-methyl-4-pyridinol nitrate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-methyl-4-pyridinol nitrate

There total 1 articles about 2-methyl-4-pyridinol nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-66-6
2-methyl-4-nitropyridine N-oxide

: 18614-65-8
2-methyl-4-pyridinol nitrate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / acetic acid / 2068.6 Torr

2: 40 percent / HNO₃, NaNO₂ / H₂O / <20 deg C

With hydrogen; nitric acid; sodium nitrite; platinum(IV) oxide; In water; acetic acid;
DOI:10.1021/jm00131a010

Reference yield:

: 18614-65-8
2-methyl-4-pyridinol nitrate

: 486-84-0
harmane

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid; sulfuric acid / 0 - 130 °C

1.2: 10 h / Reflux; Inert atmosphere

2.1: copper; copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / dimethyl sulfoxide / 0.75 h / 50 °C / Inert atmosphere

2.2: 6.66 h / Inert atmosphere

3.1: palladium on activated carbon; hydrogen / methanol / 16 h / 22 °C

4.1: palladium on activated carbon / diphenylether / 0.66 h / 210 °C / Inert atmosphere

With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; palladium on activated carbon; hydrogen; nitric acid; copper; In methanol; diphenylether; dimethyl sulfoxide; 2.1: |Ullmann Condensation / 2.2: |Ullmann Condensation;
DOI:10.1021/acs.joc.7b00323

Reference yield:

: 18614-65-8
2-methyl-4-pyridinol nitrate

: 121845-73-6
5-methylpyrido[3,4-e]-1,2,4-triazine

Guidance literature:: Multi-step reaction with 6 steps

1: HNO₃, H₂SO₄ / 2 h / Heating

2: 26.7 g / POCl₃ / 2 h / Heating

3: N₂H₄*H₂O / ethanol / 1.) 0 deg C, 0.75 h, 2.) 25 deg C, 3.5 h

4: H₂ / 5percent Pd/C / aq. ethanol

5: conc. HCl / 2.5 h

6: MnO₂, 5 M NaOH / H₂O / 0.83 h / pH 6

With hydrogenchloride; manganese(IV) oxide; sodium hydroxide; sulfuric acid; hydrogen; nitric acid; hydrazine hydrate; trichlorophosphate; palladium on activated charcoal; In ethanol; water;
DOI:10.1021/jm00131a010