4-Chloro-2-methyl-3-nitropyridine

Base Information

Chemical Name:4-Chloro-2-methyl-3-nitropyridine
CAS No.:23056-35-1
Molecular Formula:C6H5ClN2O2
Molecular Weight:172.571
Hs Code.:2933399090
DSSTox Substance ID:DTXSID60560397
Wikidata:Q82443534
Mol file:23056-35-1.mol

Synonyms:4-Chloro-2-methyl-3-nitropyridine;23056-35-1;4-CHLORO-2-METHYL-3-NITRO-PYRIDINE;Pyridine, 4-chloro-2-methyl-3-nitro-;MFCD11215572;SCHEMBL2972185;DTXSID60560397;YAA05635;ZB0091;AKOS006307199;SB52912;AM803559;DS-15492;SY021422;CS-0147960;EN300-195246;A878341;J-514963;4-Chloro-2-methyl-3-nitro-pyridine

Suppliers and Price of 4-Chloro-2-methyl-3-nitropyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Chloro-2-methyl-3-nitropyridine
100mg
$ 175.00

SynQuest Laboratories
4-Chloro-2-methyl-3-nitropyridine 95%
1 g
$ 1040.00

SynQuest Laboratories
4-Chloro-2-methyl-3-nitropyridine 95%
250 mg
$ 480.00

Crysdot
4-Chloro-2-methyl-3-nitropyridine 95+%
1g
$ 432.00

Crysdot
4-Chloro-2-methyl-3-nitropyridine 95+%
5g
$ 1382.00

Chemenu
4-Chloro-2-methyl-3-nitropyridine 95%
5g
$ 1305.00

Chemenu
4-Chloro-2-methyl-3-nitropyridine 95%
1g
$ 408.00

Apolloscientific
4-Chloro-2-methyl-3-nitropyridine 95%
250mg
$ 435.00

Apolloscientific
4-Chloro-2-methyl-3-nitropyridine 95%
1g
$ 943.00

American Custom Chemicals Corporation
4-CHLORO-2-METHYL-3-NITROPYRIDINE 95.00%
5MG
$ 496.75

Total 20 raw suppliers

Chemical Property of 4-Chloro-2-methyl-3-nitropyridine

Chemical Property:

Melting Point:45-48 °C
Boiling Point:247.1±35.0 °C(Predicted)
PKA:1.58±0.10(Predicted)
PSA：58.71000
Density:1.406±0.06 g/cm3(Predicted)
LogP:2.47480
Storage Temp.:Inert atmosphere,Store in freezer, under -20°C
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:172.0039551
Heavy Atom Count:11
Complexity:159

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-2-methyl-3-nitropyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC=CC(=C1[N+](=O)[O-])Cl

Technology Process of 4-Chloro-2-methyl-3-nitropyridine

There total 6 articles about 4-Chloro-2-methyl-3-nitropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-66-6
2-methyl-4-nitropyridine N-oxide

: 23056-35-1
4-chloro-2-methyl-3-nitropyridine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / PtO₂ / acetic acid / 2068.6 Torr

2: 40 percent / HNO₃, NaNO₂ / H₂O / <20 deg C

3: HNO₃, H₂SO₄ / 2 h / Heating

4: 26.7 g / POCl₃ / 2 h / Heating

With sulfuric acid; hydrogen; nitric acid; sodium nitrite; trichlorophosphate; platinum(IV) oxide; In water; acetic acid;
DOI:10.1021/jm00131a010

Reference yield:

: 18614-66-9
2-methyl-3-nitro-4-pyridinol

: 10026-13-8,874483-75-7
phosphorus pentachloride

: 23056-35-1
4-chloro-2-methyl-3-nitropyridine

Guidance literature:: In dichloromethane; trichlorophosphate;

Reference yield:

: 18437-58-6
3-methyl-4-pyridinamine

: 23056-35-1
4-chloro-2-methyl-3-nitropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / HNO₃, NaNO₂ / H₂O / <20 deg C

2: HNO₃, H₂SO₄ / 2 h / Heating

3: 26.7 g / POCl₃ / 2 h / Heating

With sulfuric acid; nitric acid; sodium nitrite; trichlorophosphate; In water;
DOI:10.1021/jm00131a010