(S)-4,6-Bis-benzyloxy-hexanal

Base Information

Chemical Name:(S)-4,6-Bis-benzyloxy-hexanal
CAS No.:104784-36-3
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

Synonyms:(S)-4,6-Bis-benzyloxy-hexanal

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Chemical Property of (S)-4,6-Bis-benzyloxy-hexanal

Chemical Property:

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Technology Process of (S)-4,6-Bis-benzyloxy-hexanal

There total 7 articles about (S)-4,6-Bis-benzyloxy-hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104784-34-1
2-<(3S)-3,5-dibenzyloxypentyl>-1,3-dithiane

: 104784-36-3
(S)-4,6-Bis-benzyloxy-hexanal

Guidance literature:: With boron trifluoride; mercury(II) oxide; In tetrahydrofuran; water; acetone; for 20h;
DOI:10.1016/0008-6215(86)80035-0

Reference yield:

: 100-39-0
benzyl bromide

: 104784-36-3
(S)-4,6-Bis-benzyloxy-hexanal

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / 50percent sodium hydride / tetrahydrofuran / 1 h / Ambient temperature

2: 80 percent / boron trifluoride etherate / CH₂Cl₂ / 2 h / Ambient temperature

3: 1.)sodium hydride / 1.) THF, 1 h, 2.) RT, 24 h

4: 96 percent / α,α-azobisisobutyronitrile, tributyltin hydride / toluene / 18 h / Heating

5: red mercuric oxide, boron trifluoride / acetone; H₂O; tetrahydrofuran / 20 h

With azobisisobutyronitrile; boron trifluoride diethyl etherate; boron trifluoride; tri-n-butyl-tin hydride; sodium hydride; mercury(II) oxide; In tetrahydrofuran; dichloromethane; water; acetone; toluene;
DOI:10.1016/0008-6215(86)80035-0

Reference yield:

: 104784-32-9
(2R,3S,6S)-6-ethoxy-3-phenylmethoxy-2-phenylmethoxymethyltetrahydropyran

: 104784-36-3
(S)-4,6-Bis-benzyloxy-hexanal

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / boron trifluoride etherate / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.)sodium hydride / 1.) THF, 1 h, 2.) RT, 24 h

3: 96 percent / α,α-azobisisobutyronitrile, tributyltin hydride / toluene / 18 h / Heating

4: red mercuric oxide, boron trifluoride / acetone; H₂O; tetrahydrofuran / 20 h

With azobisisobutyronitrile; boron trifluoride diethyl etherate; boron trifluoride; tri-n-butyl-tin hydride; sodium hydride; mercury(II) oxide; In tetrahydrofuran; dichloromethane; water; acetone; toluene;
DOI:10.1016/0008-6215(86)80035-0