Technology Process of ethyl (S)-6,8-dibenzyloxyoct-2-enoate
There total 8 articles about ethyl (S)-6,8-dibenzyloxyoct-2-enoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 89 percent / 50percent sodium hydride / tetrahydrofuran / 1 h / Ambient temperature
2: 80 percent / boron trifluoride etherate / CH2Cl2 / 2 h / Ambient temperature
3: 1.)sodium hydride / 1.) THF, 1 h, 2.) RT, 24 h
4: 96 percent / α,α-azobisisobutyronitrile, tributyltin hydride / toluene / 18 h / Heating
5: red mercuric oxide, boron trifluoride / acetone; H2O; tetrahydrofuran / 20 h
6: 80 percent / benzene / 10 h / Heating
With
azobisisobutyronitrile; boron trifluoride diethyl etherate; boron trifluoride; tri-n-butyl-tin hydride; sodium hydride; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane; water; acetone; toluene; benzene;
DOI:10.1016/0008-6215(86)80035-0
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / boron trifluoride etherate / CH2Cl2 / 2 h / Ambient temperature
2: 1.)sodium hydride / 1.) THF, 1 h, 2.) RT, 24 h
3: 96 percent / α,α-azobisisobutyronitrile, tributyltin hydride / toluene / 18 h / Heating
4: red mercuric oxide, boron trifluoride / acetone; H2O; tetrahydrofuran / 20 h
5: 80 percent / benzene / 10 h / Heating
With
azobisisobutyronitrile; boron trifluoride diethyl etherate; boron trifluoride; tri-n-butyl-tin hydride; sodium hydride; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane; water; acetone; toluene; benzene;
DOI:10.1016/0008-6215(86)80035-0
