sodium 2,6-dimethylbenzoate

Base Information

• Chemical Name: sodium 2,6-dimethylbenzoate
• CAS No.: 69795-09-1
• Molecular Formula: C₉H₉O₂*Na
• Molecular Weight: 172.159
• Mol file: 69795-09-1.mol

Synonyms:sodium 2,6-dimethylbenzoate

Chemical Property of sodium 2,6-dimethylbenzoate

Chemical Property:

Purity/Quality:

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Technology Process of sodium 2,6-dimethylbenzoate

There total 1 articles about sodium 2,6-dimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2,6-dimethylbenzoate (14920-81-1) + sodium benzylmercaptide (3492-64-6) → [(methylthio)methyl]-benzene (766-92-7) + sodium 2,6-dimethylbenzoate (69795-09-1)

Guidance literature:

In water; N,N-dimethyl-formamide; at 35 ℃; Rate constant; benzenemethanethiolates of other alkali metals;

DOI:10.1002/recl.19931120607

Reference yield:

1-chloromenth-2-ene + 2,6-dimethylbenzoic acid (632-46-2) + sodium 2,6-dimethylbenzoate (69795-09-1) → C19H26O2

Guidance literature:

In N,N-dimethyl-formamide; at 120 ℃; for 12h;

Reference yield:

copper(II) sulfate (7758-99-8) + sodium 2,6-dimethylbenzoate (69795-09-1) → copper(II) 2,6-dimethylbenzoate

Guidance literature:

In water; slight excess of aq. CuSO4 soln. added to soln. of the organic compoundwith stirring; filtered, washed with distilled H2O, dried over anhydrous CaCl2 in a vacuum desiccator at room temp., dried in a vacuum pistol between 100 and 110°C over P2O5, elem. anal.;

DOI:10.1016/0022-1902(81)80420-4

upstream raw materials:

methyl 2,6-dimethylbenzoate

sodium benzylmercaptide

Refernces