Benzeneethanimidoyl chloride, N-hydroxy-alpha-oxo-, (Z)- (9CI)

Base Information

• Chemical Name: Benzeneethanimidoyl chloride, N-hydroxy-alpha-oxo-, (Z)- (9CI)
• CAS No.: 17019-28-2
• Molecular Formula: C8H6 Cl N O2
• Molecular Weight: 183.594
• Mol file: 17019-28-2.mol

Synonyms:Benzeneethanimidoylchloride, N-hydroxy-a-oxo-, (Z)- (9CI); Glyoxylohydroximoyl chloride, 2-phenyl-, (Z)- (8CI)

Chemical Property of Benzeneethanimidoyl chloride, N-hydroxy-alpha-oxo-, (Z)- (9CI)

Chemical Property:

• PSA: 49.66000
• LogP: 1.89580

Purity/Quality:

99% ^*data from raw suppliers

(1Z)-N-HYDROXY-2-OXO-2-PHENYLETHANIMIDOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneethanimidoyl chloride, N-hydroxy-alpha-oxo-, (Z)- (9CI)

There total 6 articles about Benzeneethanimidoyl chloride, N-hydroxy-alpha-oxo-, (Z)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

acetophenone (98-86-2) → (Z)-N-hydroxy-α-oxobenzeneethanimidoyl chloride (17019-28-2)

Guidance literature:

With hydrogenchloride; nitric acid; sodium nitrite; In water; at 70 ℃; for 1.75h;

DOI:10.1002/(SICI)1522-2675(19990804)82:8<1289::AID-HLCA1289>3.0.CO;2-W

Reference yield: 20.0%

t-butyl thionitrite (15459-95-7) + 1-chloroacetophenone (532-27-4,108321-66-0,164322-25-2) → 2-methylpropan-2-thiol (75-66-1) + (Z)-N-hydroxy-α-oxobenzeneethanimidoyl chloride (17019-28-2)

Guidance literature:

In diethyl ether; at 25 ℃; for 3h;

DOI:10.1016/S0040-4039(01)82909-9

Reference yield:

1-chloroacetophenone (532-27-4,108321-66-0,164322-25-2) → (Z)-N-hydroxy-α-oxobenzeneethanimidoyl chloride (17019-28-2)

Guidance literature:

With isopentyl nitrite;

upstream raw materials:

oxo-phenyl-acetaldehyde oxime

phenylglyoxylonitrile oxide

1-chloroacetophenone

t-butyl thionitrite

Downstream raw materials:

(4-nitro-5-phenylisoxazol-3-yl)(phenyl)methanone

3-benzoyl-5-butoxy-4,5-dihydroisoxazole

isoxazol-3-yl(phenyl)methanone

methyl 2-oxo-2-phenylacetate

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