C₁₂H₁₈BrO₄P

Base Information

Chemical Name:C₁₂H₁₈BrO₄P
CAS No.:1242319-64-7
Molecular Formula:C₁₂H₁₈BrO₄P
Molecular Weight:337.15
Hs Code.:

C<sub>12</sub>H<sub>18</sub>BrO<sub>4</sub>P

Synonyms:C₁₂H₁₈BrO₄P

Suppliers and Price of C₁₂H₁₈BrO₄P

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₂H₁₈BrO₄P

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₂H₁₈BrO₄P

There total 5 articles about C₁₂H₁₈BrO₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 762-04-9
phosphonic acid diethyl ester

: 126712-05-8
1-bromo-2-(bromomethyl)-3-methoxybenzene

: 1242319-64-7
C₁₂H₁₈BrO₄P

Guidance literature:: phosphonic acid diethyl ester; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.25h; Inert atmosphere;

1-bromo-2-(bromomethyl)-3-methoxybenzene; In tetrahydrofuran; toluene; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1002/anie.201002264

Reference yield:

: 126712-07-0
2-bromo-6-methoxybenzaldehyde

: 1242319-64-7
C₁₂H₁₈BrO₄P

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

2.1: phosphorus tribromide / pyridine / diethyl ether / 4 h / 25 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

3.2: 12 h / 25 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium hexamethylsilazane; pyridine; In tetrahydrofuran; methanol; diethyl ether; toluene;

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 1242319-64-7
C₁₂H₁₈BrO₄P

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / 24 h / 25 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 8 h / -40 - -20 °C / Inert atmosphere

2.2: 12 h / 0 - 25 °C

2.3: 1 h / 0 °C

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

4.1: phosphorus tribromide / pyridine / diethyl ether / 4 h / 25 °C / Inert atmosphere

5.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

5.2: 12 h / 25 °C

With sodium tetrahydroborate; tert.-butyl lithium; phosphorus tribromide; potassium hexamethylsilazane; pyridine; In tetrahydrofuran; methanol; diethyl ether; ethanol; toluene; pentane;