3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

Base Information

Chemical Name:3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione
CAS No.:109619-77-4
Molecular Formula:C₂₀H₂₀Br₂N₂O₄
Molecular Weight:512.198
Hs Code.:

Synonyms:3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

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Chemical Property of 3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

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Technology Process of 3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

There total 5 articles about 3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 109619-74-1
6-benzylidene-3-α-bromobenzyl-3-hydroxy-1-methyl-2,5-piperazinedione

: 109619-77-4
3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

Guidance literature:: With N-Bromosuccinimide; In chloroform; for 3h; Ambient temperature;
DOI:10.1246/cl.1986.1453

Reference yield:

: 100-52-7
benzaldehyde

: 109619-77-4
3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 5 steps

1: t-BuOK

3: 98 percent / t-BuOK

4: 95 percent / water, N-bromosuccinimide

5: 70 percent / N-bromosuccinimide / CHCl₃ / 3 h / Ambient temperature

With N-Bromosuccinimide; potassium tert-butylate; water; In chloroform;
DOI:10.1246/cl.1986.1453

Reference yield:

: 80687-66-7
(Z)-1-acetyl-3-benzylidene-4-methylpiperazine-2,5-dione

: 109619-77-4
3,6-di(α-bromobenzyl)-3-hydroxy-6-methoxy-1-methyl-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / t-BuOK

2: 95 percent / water, N-bromosuccinimide

3: 70 percent / N-bromosuccinimide / CHCl₃ / 3 h / Ambient temperature

With N-Bromosuccinimide; potassium tert-butylate; water; In chloroform;
DOI:10.1246/cl.1986.1453