phenylisocyanoamine

Base Information

• Chemical Name: phenylisocyanoamine
• CAS No.: 61743-02-0
• Molecular Formula: C₇H₆N₂
• Molecular Weight: 118.138
• Mol file: 61743-02-0.mol

Synonyms:phenylisocyanoamine

Chemical Property of phenylisocyanoamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of phenylisocyanoamine

There total 2 articles about phenylisocyanoamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-[1,3]dioxane-4,5,6-trione-5-phenylhydrazone (75307-67-4) → phenylisocyanoamine (61743-02-0) + 1-phenylcyanamide (622-34-4)

Guidance literature:

In gas; at 400 ℃; under 0.0001 - 0.001 Torr; Title compound not separated from byproducts;

DOI:10.1021/jo00189a025

Reference yield:

phenylhydrazine (100-63-0) → phenylisocyanoamine (61743-02-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / ethanol / 1 h / Ambient temperature

2: gas / 400 °C / 0 - 0 Torr

In ethanol;

DOI:10.1021/jo00189a025

upstream raw materials:

2,2-dimethyl-[1,3]dioxane-4,5,6-trione-5-phenylhydrazone

phenylhydrazine