4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

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Chemical Name:4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile
CAS No.:1319065-27-4
Molecular Formula:C₂₃H₁₈N₈O
Molecular Weight:422.449
Hs Code.:

Synonyms:4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

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Chemical Property of 4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

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Technology Process of 4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

There total 4 articles about 4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1443-80-7
4-cyanophenyl methyl ketone

: 1319067-61-2
N₃-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-1H-[1,2,4]triazole-3,5-diamine

: 1319065-27-4
4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

Guidance literature:: 4-cyanophenyl methyl ketone; With tert-Butoxybis(dimethylamino)methane; In 1,4-dioxane; for 4h; Reflux;

N₃-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-1H-[1,2,4]triazole-3,5-diamine; With acetic acid; at 100 ℃;

Reference yield: 72.0%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 1443-80-7
4-cyanophenyl methyl ketone

: 1319067-61-2
N₃-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-1H-[1,2,4]triazole-3,5-diamine

: 1319065-27-4
4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

Guidance literature:: tert-Butoxybis(dimethylamino)methane; 4-cyanophenyl methyl ketone; In 1,4-dioxane; for 4h; Reflux;

N₃-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-1H-[1,2,4]triazole-3,5-diamine; With acetic acid; In 1,4-dioxane; at 100 ℃;

Reference yield:

: 958245-18-6
3-methoxy-4-(4-methyl-1H-imidazol-1-yl)aniline

: 1319065-27-4
4-{2-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenylamino]-[1,2,4]triazolo[1,5-a]pyrimidin-7-yl}-benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropyl alcohol / 2 h / 20 °C

2.1: hydrazine hydrate / methanol / 1 h / 20 °C

3.1: 1,4-dioxane / 4 h / Reflux

3.2: 100 °C

With hydrazine hydrate; In 1,4-dioxane; methanol; isopropyl alcohol;