1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Base Information

Chemical Name:1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione
CAS No.:628718-11-6
Molecular Formula:C₁₇H₂₁BrN₂O₆
Molecular Weight:429.268
Hs Code.:

Synonyms:1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Technology Process of 1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

There total 4 articles about 1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 628718-04-7
1-Acetyl-3-[1-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: 628718-11-6
1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: With hydrogen; Rh on carbon; In isopropyl alcohol; for 19h; under 760 Torr;
DOI:10.1248/cpb.51.821

Reference yield:

: 3027-05-2
N,N'-diacetylpiperazin-2,5-dione

: 628718-11-6
1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 6.749 g / potassium tert-butoxide / 2-methyl-propan-2-ol; dimethylformamide / 1 h / 25 °C

2: 100 percent / H₂ / Rh/C / propan-2-ol / 19 h / 760 Torr

With potassium tert-butylate; hydrogen; Rh on carbon; In N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol;
DOI:10.1248/cpb.51.821

Reference yield:

: 287117-31-1
2-bromo-5-hydroxy-4-methoxy-3-methylbenzaldehyde

: 628718-11-6
1-acetyl-3-(2-bromo-4-methoxy-5-methoxymethoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 1 h / 25 °C

2: 6.749 g / potassium tert-butoxide / 2-methyl-propan-2-ol; dimethylformamide / 1 h / 25 °C

3: 100 percent / H₂ / Rh/C / propan-2-ol / 19 h / 760 Torr

With potassium tert-butylate; hydrogen; potassium carbonate; Rh on carbon; In N,N-dimethyl-formamide; isopropyl alcohol; tert-butyl alcohol;
DOI:10.1248/cpb.51.821