3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one

Base Information

Chemical Name:3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one
CAS No.:32059-76-0
Molecular Formula:C₂₂H₁₇NO
Molecular Weight:311.383
Hs Code.:
DSSTox Substance ID:DTXSID801212806

Synonyms:DTXSID801212806;3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one;32059-76-0

Suppliers and Price of 3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:311.131014166
Heavy Atom Count:24
Complexity:478

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)C=CC(=O)C3=CC=CC=C3)C4=CC=CC=C41

Technology Process of 3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one

There total 4 articles about 3-(9-Methyl-9H-carbazol-3-yl)-1-phenyl-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21240-56-2
9-methyl-9H-carbazole-3-carbaldehyde

: 98-86-2
acetophenone

: 32059-76-0
3-(9-methyl-9H-carbazol-3-yl)-1-phenylpropenone

Guidance literature:: With sodium hydroxide; In ethanol; water; at 0 - 20 ℃;
DOI:10.3109/14756366.2012.663365

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 32059-76-0
3-(9-methyl-9H-carbazol-3-yl)-1-phenylpropenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

1.2: 3 h / 20 °C

2.1: trichlorophosphate / 4 h / 0 - 80 °C

3.1: sodium hydroxide / ethanol; water / 0 - 20 °C

With sodium hydride; sodium hydroxide; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; 2.1: |Vilsmeier-Haack Formylation / 3.1: |Claisen-Schmidt Condensation;
DOI:10.3109/14756366.2012.663365

Reference yield:

: 1484-12-4
N-methylcarbazole

: 32059-76-0
3-(9-methyl-9H-carbazol-3-yl)-1-phenylpropenone

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 4 h / 0 - 80 °C

2: sodium hydroxide / ethanol; water / 0 - 20 °C

With sodium hydroxide; trichlorophosphate; In ethanol; water; 1: |Vilsmeier-Haack Formylation / 2: |Claisen-Schmidt Condensation;
DOI:10.3109/14756366.2012.663365