N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

Base Information

Chemical Name:N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine
CAS No.:103185-60-0
Molecular Formula:C₁₄H₁₃ClN₂O
Molecular Weight:260.723
Hs Code.:

Synonyms:N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

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Technology Process of N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

There total 1 articles about N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 104-88-1
4-chlorobenzaldehyde

: 3471-32-7
4-Methoxyphenylhydrazine

: 103185-60-0
N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

Guidance literature:: With sodium acetate; In ethanol; for 2h; Reflux;
DOI:10.3390/molecules25215013

Reference yield: 83.0%

: 101671-00-5,5153-68-4
(E)-2-(4-methylphenyl)-1-nitroethene

: 103185-60-0
N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

: 1016169-41-7
3-(4-chloro-phenyl)-1-(4-methoxy-phenyl)-4-p-tolyl-1H-pyrazole

Guidance literature:: N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

(E)-2-(4-methylphenyl)-1-nitroethene; at -78 ℃; for 0.25h; Inert atmosphere;

With trifluoroacetic acid; In tetrahydrofuran; at -78 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol800200j

Reference yield: 72.0%

: 56-23-5
tetrachloromethane

: 103185-60-0
N-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-N'-(4-methoxy-phenyl)-hydrazine

: C₁₅H₁₁Cl₃N₂O

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; copper(l) chloride; In dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.3390/molecules25215013