UNC₉₉₇₅

Base Information

Chemical Name:UNC₉₉₇₅
CAS No.:1354030-19-5
Molecular Formula:C₂₃H₂₈Cl₂N₄O₂
Molecular Weight:463.407
Hs Code.:

Synonyms:UNC₉₉₇₅

Suppliers and Price of UNC₉₉₇₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of UNC₉₉₇₅

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of UNC₉₉₇₅

There total 11 articles about UNC₉₉₇₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1354030-18-4
4-(7-oxo-5,6,7,8-tetrahydro-1,8-naphthyridin-2-yloxy)butyl methanesulfonate

: 839712-09-3
1-(2,3-dichlorophenyl)-1,4-diazepane hydrochloride

: 1354030-19-5
UNC₉₉₇₅

Guidance literature:: With triethylamine; sodium iodide; In acetonitrile; at 70 ℃;

Reference yield:

: 45644-21-1
6-chloropyridin-2-amine

: 1354030-19-5
UNC₉₉₇₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / dichloromethane / 20 °C / Cooling with ice

2.1: n-butyllithium / tetrahydrofuran / 3 h / -20 °C

2.2: -20 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

4.1: sodium hydride / tetrahydrofuran / Inert atmosphere; Cooling with ice

4.2: Reflux

5.1: hydrogen / Raney nickel / tetrahydrofuran

6.1: hydrogenchloride / 1,4-dioxane / 3 h / Reflux

6.2: 20 °C / pH 8

7.1: hydrogen / palladium 10% on activated carbon / ethanol

8.1: triethylamine / dichloromethane / 6 h / 20 °C

9.1: triethylamine; sodium iodide / acetonitrile / 70 °C

With hydrogenchloride; n-butyllithium; hydrogen; sodium hydride; triethylamine; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 86847-84-9
2,2-Dimethyl-N-(6-chloro-2-pyridinyl)propanamide

: 1354030-19-5
UNC₉₉₇₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran / 3 h / -20 °C

1.2: -20 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

3.1: sodium hydride / tetrahydrofuran / Inert atmosphere; Cooling with ice

3.2: Reflux

4.1: hydrogen / Raney nickel / tetrahydrofuran

5.1: hydrogenchloride / 1,4-dioxane / 3 h / Reflux

5.2: 20 °C / pH 8

6.1: hydrogen / palladium 10% on activated carbon / ethanol

7.1: triethylamine / dichloromethane / 6 h / 20 °C

8.1: triethylamine; sodium iodide / acetonitrile / 70 °C

With hydrogenchloride; n-butyllithium; hydrogen; sodium hydride; triethylamine; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;