N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

Base Information

Chemical Name:N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal
CAS No.:130627-35-9
Molecular Formula:C₂₃H₂₆N₂O₅S
Molecular Weight:442.536
Hs Code.:

Synonyms:N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

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Chemical Property of N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

Chemical Property:

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Technology Process of N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

There total 5 articles about N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 140858-28-2
2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

: 540-51-2
2-bromoethanol

: 130627-35-9
N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

Guidance literature:: With potassium carbonate; In ethanol; for 15h; Heating;
DOI:10.1021/jo00022a015

Reference yield:

: 62240-37-3
2-(2-methyl-1,3-dioxolane-2-yl)ethan-1-amine

: 130627-35-9
N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / benzene / a.) 0 deg C, 15 min, b.) r. t., overnight, c.) 19 h, reflux

2: 72 percent / p-TsOH / benzene / 1 h / Heating

3: 62 percent / K₂CO₃ / ethanol / 15 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In ethanol; benzene;
DOI:10.1021/jo00022a015

Reference yield:

: 80360-20-9
1-(phenylsulfonyl)indole-3-carbaldehyde

: 130627-35-9
N-(2-hydroxyethyl)-2-<1-(phenylsulfonyl)-3-indolyl>-4-piperidone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / benzene / a.) 0 deg C, 15 min, b.) r. t., overnight, c.) 19 h, reflux

2: 72 percent / p-TsOH / benzene / 1 h / Heating

3: 62 percent / K₂CO₃ / ethanol / 15 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In ethanol; benzene;
DOI:10.1021/jo00022a015