methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

Base Information

Chemical Name:methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate
CAS No.:1426054-32-1
Molecular Formula:C₁₈H₁₁Cl₂F₃N₂O₅
Molecular Weight:463.197
Hs Code.:

Synonyms:methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

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Chemical Property of methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

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Technology Process of methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

There total 3 articles about methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1424279-71-9
methyl 4-hydroxyiminomethyl-2-nitrobenzoate

: 1426054-32-1
methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

Guidance literature:: methyl 4-hydroxyiminomethyl-2-nitrobenzoate; With N-chloro-succinimide; In N,N-dimethyl-formamide; at 50 ℃; for 3h; Inert atmosphere;

1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 1424279-70-8
methyl 4-dimethoxymethyl-2-nitrobenzoate

: 1426054-32-1
methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / acetone / 2 h

2.1: sodium acetate; hydroxylamine hydrochloride / isopropyl alcohol; water / 2 h / 20 °C

3.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

3.2: 16 h / 20 °C

With hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; In water; N,N-dimethyl-formamide; isopropyl alcohol; acetone;

Reference yield:

: methyl 4-formyl-2-nitro benzoate

: 1426054-32-1
methyl 4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate; hydroxylamine hydrochloride / isopropyl alcohol; water / 2 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

2.2: 16 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; In water; N,N-dimethyl-formamide; isopropyl alcohol;