(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

Base Information

Chemical Name:(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester
CAS No.:944913-95-5
Molecular Formula:C₁₉H₂₈N₂O₃
Molecular Weight:332.443
Hs Code.:

Synonyms:(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

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Chemical Property of (4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

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Technology Process of (4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

There total 9 articles about (4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₁₉H₂₆N₂O₃

: 944913-95-5
(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c2ob26828k

Reference yield: 84.0%

: 944913-91-1
(S)-1-benzyl-4-[(Z)-tert-butyloxycarbonylmethylidene]-5-(1-methylethyl)-imidazolidin-2-one

: 944913-95-5
(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane; at -78 - 20 ℃; for 1.75h;
DOI:10.1021/ol0708020

Reference yield: 84.0%

: 67-56-1
methanol

: 944913-91-1
(S)-1-benzyl-4-[(Z)-tert-butyloxycarbonylmethylidene]-5-(1-methylethyl)-imidazolidin-2-one

: 944913-95-5
(4R,5S)-5-(1-methylethyl)-1-phenylmethyl-2-oxo-imidazolidin-4-acetic acid tert-butyl ester

: 1159813-81-6
C₁₆H₂₂N₂O₃

Guidance literature:: With hydrogenchloride; bromocresol green; sodium cyanoborohydride; In dichloromethane; at -78 - 20 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo900324d