C₂₆H₂₄Cl₂O₉

Base Information

• Chemical Name: C₂₆H₂₄Cl₂O₉
• CAS No.: 1314917-94-6
• Molecular Formula: C₂₆H₂₄Cl₂O₉
• Molecular Weight: 551.377
• Mol file: 1314917-94-6.mol

Synonyms:C₂₆H₂₄Cl₂O₉

Chemical Property of C₂₆H₂₄Cl₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₄Cl₂O₉

There total 6 articles about C₂₆H₂₄Cl₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-hydroxy-3,6,7-tris(methoxymethoxy)-9H-xanthen-9-one (1314917-55-9) + 2,4-dichlorobenzyl bromide (20443-99-6) → C26H24Cl2O9 (1314917-94-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 6h;

DOI:10.1016/j.bmcl.2011.04.140

Reference yield:

2,4,5-trimethoxybenzoyl chloride (42833-66-9) → C26H24Cl2O9 (1314917-94-6)

Guidance literature:

Multi-step reaction with 5 steps

1: aluminum (III) chloride / diethyl ether / 48 h / 20 °C

2: pyridine; tetra(n-butyl)ammonium hydroxide / water / 4 h / Reflux

3: pyridine hydrochloride

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 6 h / 50 °C

With pyridine; aluminum (III) chloride; tetra(n-butyl)ammonium hydroxide; pyridine hydrochloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 1: Friedel Crafts acylation;

DOI:10.1016/j.bmcl.2011.04.140

Reference yield:

asaronic acid (490-64-2) → C26H24Cl2O9 (1314917-94-6)

Guidance literature:

Multi-step reaction with 6 steps

1: thionyl chloride / Reflux

2: aluminum (III) chloride / diethyl ether / 48 h / 20 °C

3: pyridine; tetra(n-butyl)ammonium hydroxide / water / 4 h / Reflux

4: pyridine hydrochloride

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

6: potassium carbonate / N,N-dimethyl-formamide / 6 h / 50 °C

With pyridine; aluminum (III) chloride; thionyl chloride; tetra(n-butyl)ammonium hydroxide; pyridine hydrochloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; 2: Friedel Crafts acylation;

DOI:10.1016/j.bmcl.2011.04.140

upstream raw materials:

1-hydroxy-3,6,7-tris(methoxymethoxy)-9H-xanthen-9-one

2,4-dichlorobenzyl bromide

2,4,5-trimethoxybenzoyl chloride

asaronic acid

Downstream raw materials:

C₂₀H₁₂Cl₂O₆