3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

Base Information

Chemical Name:3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide
CAS No.:1449521-91-8
Molecular Formula:C₂₃H₄₃NO₄Si₂
Molecular Weight:453.77
Hs Code.:

Synonyms:3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

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Technology Process of 3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

There total 4 articles about 3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₄₂O₄Si₂

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1449521-91-8
3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

Guidance literature:: With isopropylmagnesium chloride; In tetrahydrofuran; at -40 ℃; for 0.416667h;
DOI:10.1016/j.tetlet.2013.05.044

Reference yield:

: 2881-83-6
ethyl 4-methoxybenzoylacetate

: 1449521-91-8
3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane / 3.5 h / -78 - -15 °C

2: sodium tetrahydroborate; ethanol / 3 h / 0 °C

3: 1H-imidazole / dichloromethane / 18 h / 23 °C

4: isopropylmagnesium chloride / tetrahydrofuran / 0.42 h / -40 °C

With 1H-imidazole; sodium tetrahydroborate; ethanol; isopropylmagnesium chloride; boron tribromide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.05.044

Reference yield:

: 77103-47-0
ethyl (4-hydroxybenzoyl)acetate

: 1449521-91-8
3-(tert-butyldimethylsilyloxy)-3-(4-(tert-butyldimethylsilyloxy) phenyl)-N-methoxy-N-methylpropanamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; ethanol / 3 h / 0 °C

2: 1H-imidazole / dichloromethane / 18 h / 23 °C

3: isopropylmagnesium chloride / tetrahydrofuran / 0.42 h / -40 °C

With 1H-imidazole; sodium tetrahydroborate; ethanol; isopropylmagnesium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.05.044