3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

Base Information

Chemical Name:3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether
CAS No.:1025691-25-1
Molecular Formula:C₁₇H₂₈OSi₂
Molecular Weight:304.58
Hs Code.:

Synonyms:3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

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Chemical Property of 3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

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Technology Process of 3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

There total 1 articles about 3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-77-4
chloro-trimethyl-silane

: 930-68-7
cyclohexenone

: 768-33-2
phenyldimethylsilyl chloride

: 1025691-25-1
3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

Guidance literature:: phenyldimethylsilyl chloride; With lithium; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;

With copper(l) iodide; In tetrahydrofuran; at -25 ℃; for 4h; Inert atmosphere;

chloro-trimethyl-silane; cyclohexenone; With triethylamine; In tetrahydrofuran; at -25 - 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2016.05.063

Reference yield: 31.0%

: 1025691-25-1
3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

: 82202-13-9
3-dimethylphenylsilyl-2-cyclohexen-1-one

Guidance literature:: With air; In toluene; at 110 ℃; for 10h;
DOI:10.1021/ol800007v

Reference yield:

: 1126-76-7
1,2-Epoxy-4-phenylbutane

: 1025691-25-1
3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether

: C₂₄H₃₂O₂Si

Guidance literature:: 3-dimethylphenylsilyl-1-cyclohexenyl trimethylsilyl ether; With methyllithium; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.0833333h; Inert atmosphere;

1,2-Epoxy-4-phenylbutane; With boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2016.05.063