trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate

Base Information

Chemical Name:trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate
CAS No.:166041-12-9
Molecular Formula:C₁₇H₁₆MnN₂O₅*ClO₄*H₂O
Molecular Weight:500.728
Hs Code.:

Synonyms:trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate

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Chemical Property of trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate

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Technology Process of trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate

There total 1 articles about trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 366-18-7
[2,2]bipyridinyl

: 35638-41-6
tetra-n-butylammonium permanganate

: 638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3
manganese triacetate

: 54-21-7
sodium salicylate

: 166041-12-9
trans-diaqua(bipyridyl)(salicylato)manganese(III) perchlorate monohydrate

Guidance literature:: In methanol; acetonitrile; simultaneously dropwise addn. solns. of Bu4NMnO4 and C10H8N2 to soln. ofMnAc3 and salicylate with stirring, stirring for 3 h, filtering, Et2O d iffusion into filtrate for 2 wk (crystn.); recrystn. (EtOH/Et2O);
DOI:10.1107/S0108270195000539