2-iodo-4,6-dimethoxybenzoic acid

Base Information

Chemical Name:2-iodo-4,6-dimethoxybenzoic acid
CAS No.:852810-81-2
Molecular Formula:C₉H₉IO₄
Molecular Weight:308.073
Hs Code.:

Synonyms:2-iodo-4,6-dimethoxybenzoic acid

Suppliers and Price of 2-iodo-4,6-dimethoxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Iodo-4,6-dimethoxybenzoicacid 97%
10g
$ 937.00

Crysdot
2-Iodo-4,6-dimethoxybenzoicacid 97%
5g
$ 653.00

Crysdot
2-Iodo-4,6-dimethoxybenzoicacid 97%
1g
$ 326.00

Crysdot
2-Iodo-4,6-dimethoxybenzoicacid 97%
25g
$ 1692.00

Alichem
2-Iodo-4,6-dimethoxybenzoicacid
25g
$ 3517.50

Alichem
2-Iodo-4,6-dimethoxybenzoicacid
10g
$ 1876.00

Alichem
2-Iodo-4,6-dimethoxybenzoicacid
5g
$ 1387.57

Total 3 raw suppliers

Chemical Property of 2-iodo-4,6-dimethoxybenzoic acid

Chemical Property:

Boiling Point:388.6±42.0 °C(Predicted)
Density:1.790±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

2-Iodo-4,6-dimethoxybenzoicacid 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-iodo-4,6-dimethoxybenzoic acid

There total 4 articles about 2-iodo-4,6-dimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 16147-09-4
2-iodo-4,6-dimethoxybenzaldehyde

: 852810-81-2
2-iodo-4,6-dimethoxybenzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; In water; acetonitrile;
DOI:10.1016/j.tetlet.2005.03.046

Reference yield:

: 25245-27-6
1-iodo-3,5-dimethoxybenzene

: 852810-81-2
2-iodo-4,6-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / POCl₃

2: 98 percent / H₂O₂; NaClO₂; NaH₂PO₄ / H₂O; acetonitrile

With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; trichlorophosphate; In water; acetonitrile; 1: Vilsmeier reaction;
DOI:10.1016/j.tetlet.2005.03.046

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 852810-81-2
2-iodo-4,6-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaNO₂; HCl / H₂O

1.2: 55 percent / KI / H₂O / Sandmeyer substitution reaction

2.1: 64 percent / POCl₃

3.1: 98 percent / H₂O₂; NaClO₂; NaH₂PO₄ / H₂O; acetonitrile

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; sodium nitrite; trichlorophosphate; In water; acetonitrile; 2.1: Vilsmeier reaction;
DOI:10.1016/j.tetlet.2005.03.046