7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

Base Information

Chemical Name:7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole
CAS No.:258839-48-4
Molecular Formula:C₁₇H₁₇N₅O₇S₂
Molecular Weight:467.483
Hs Code.:

Synonyms:7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

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Chemical Property of 7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

Chemical Property:

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Technology Process of 7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

There total 3 articles about 7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 258839-09-7
7-azidoacetylimidazo[5,1-b]thiazole

: 144-55-8
sodium hydrogencarbonate

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: 87469-14-5
2-(4-nitrobenzyloxycarbonylamino)ethanesulfonyl chloride

: 258839-48-4
7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

Guidance literature:: With hydrogenchloride; sodium hydroxide; Pd-C; In tetrahydrofuran; dichloromethane; water; hydrogen;

Reference yield:

: 251-89-8
imidazo[5,1-b]thiazole

: 258839-48-4
7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

Guidance literature:: Multi-step reaction with 3 steps

2: N-Bromosuccinimide; chloro-trimethyl-silane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; ethyl acetate; N,N-dimethyl-formamide

3: hydrogenchloride; sodium hydroxide / Pd-C / tetrahydrofuran; dichloromethane; water; hydrogen

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; chloro-trimethyl-silane; Pd-C; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; water; hydrogen; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 258838-72-1
7-acetylimidazo[5,1-b]thiazole

: 258839-48-4
7-[2-(4-Nitrobenzyloxycarbonyl)-aminoethanesulfonylamino]acetylimidazo[5,1-b]-thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; chloro-trimethyl-silane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; ethyl acetate; N,N-dimethyl-formamide

2: hydrogenchloride; sodium hydroxide / Pd-C / tetrahydrofuran; dichloromethane; water; hydrogen

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; chloro-trimethyl-silane; Pd-C; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; water; hydrogen; ethyl acetate; N,N-dimethyl-formamide;