2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

Base Information

Chemical Name:2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester
CAS No.:148743-41-3
Molecular Formula:C₁₈H₂₂N₂O₆
Molecular Weight:362.382
Hs Code.:

Synonyms:2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

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Chemical Property of 2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

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Technology Process of 2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

There total 1 articles about 2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 62965-10-0
(S)-N-carbobenzoxy-tert-butylleucine

: 148743-41-3
2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; for 12h; Ambient temperature;
DOI:10.1021/jm00045a013

Reference yield: 70.0%

: 148743-41-3
2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

: 161510-69-6
(2R,3S,4S)-N-(4-amino-2-(benzylamino)-3-hydroxy-5-phenylpentanoyl)valine benzamide

: SDZ 282457

Guidance literature:: In 1,4-dioxane; Ambient temperature;
DOI:10.1021/jm00045a013

Reference yield:

: 148743-41-3
2(S)-<<(benzyloxy)carbonyl>amino>-3,3-dimethylbutanoic acid N-hydroxysuccinimido ester

: 207121-91-3
(S)-N-benzyl 2-amino-3,3-dimethylbutanamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 8 h / 50 - 60 °C / Schlenk technique

2: hydrogen bromide / acetic acid / 20 °C / Schlenk technique

With hydrogen bromide; In tetrahydrofuran; acetic acid;
DOI:10.1039/c6ob01878e