(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Base Information

Chemical Name:(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester
CAS No.:1334513-00-6
Molecular Formula:C₁₈H₂₀N₃O₉P
Molecular Weight:453.345
Hs Code.:

Synonyms:(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

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Chemical Property of (S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Chemical Property:

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Technology Process of (S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

There total 4 articles about (S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51-28-5
2,4-Dinitrophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 39613-92-8,62062-56-0,62062-65-1
alanine isopropyl ester hydrochloride

: 1334513-00-6
(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: O-phenyl phosphorodichloridate; alanine isopropyl ester hydrochloride; With triethylamine; In dichloromethane; at -60 - -50 ℃;

2,4-Dinitrophenol; In dichloromethane; at -60 - 20 ℃;

Reference yield:

: 770-12-7
O-phenyl phosphorodichloridate

: 1334513-00-6
(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / -78 - 0 °C

2: dichloromethane / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1021/jo201492m

Reference yield:

: 51-28-5
2,4-Dinitrophenol

: 770-12-7
O-phenyl phosphorodichloridate

: 1334513-00-6
(S)-2-[(S)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

: (S)-2-[(R)-(2,4-dinitro-phenoxy)-phenoxy-phosphorylamino]propionic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / -78 - 0 °C

2: dichloromethane / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1021/jo201492m