1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane

Base Information

• Chemical Name: 1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane
• CAS No.: 2264-01-9
• Molecular Formula: C₁₂H₁₀F₈O₄
• Molecular Weight: 370.196
• Hs Code.: 29055900
• European Community (EC) Number: 671-197-4
• DSSTox Substance ID: DTXSID80379721
• Nikkaji Number: J1.593.839K
• Wikidata: Q81985809
• Mol file: 2264-01-9.mol

Synonyms:2264-01-9;1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane;2,2,3,3,4,4,5,5-octafluoro-1,6-hexyl diacrylate;1H,1H,6H,6H-Perfluorohexyldiacrylate;1H,1H,6H,6H-Perfluorohexane-1,6-diol diacrylate;(2,2,3,3,4,4,5,5-octafluoro-6-prop-2-enoyloxyhexyl) prop-2-enoate;2,2,3,3,4,4,5,5-Octafluoro-1,6-hexanediol Diacrylate;2,2,3,3,4,4,5,5-Octafluoro-1,6-hexanedioldiacrylate;2,2,3,3,4,4,5,5-octafluorohexane-1,6-diyl diacrylate;1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane (stabilized with 4-Hydroxy-TEMPO);1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane (stabilized with MEHQ);2,2,3,3,4,4,5,5-Octafluorohexamethylene Diacrylate;SCHEMBL828189;2,2,3,3,4,4,5,5-Octafluorohexan-1,6-diyl diacrylate;DTXSID80379721;BWTMTZBMAGYMOD-UHFFFAOYSA-N;MFCD00078412;AKOS016015324;FS-4645;1H,1H,6H,6H-Perfluorohexyl diacrylate;B2340;B5278;B5785;FT-0676108;1h,1h,6h,6h-perfluoro-1,6-hexyl diacrylate;D88929;1h,1h,6h,6h-perfluoro-1,6-hexanediol diacrylate;J-014792;2,2,3,3,4,4,5,5-octafluorohexane-1,6-diacrylate;1H,1H,6H,6H-Perfluorohexyldiacrylate inhibited with 50ppm 4-methoxyphenol;1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane, >/=90%,stabilized with MEHQ

Chemical Property of 1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane

Chemical Property:

• Vapor Pressure: 0.00224mmHg at 25°C
• Refractive Index: 1.378
• Boiling Point: 289.1°Cat760mmHg
• Flash Point: 124.6°C
• PSA: 52.60000
• Density: 1.383g/cm³
• LogP: 2.98600
• Solubility.: soluble in Methanol
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 11
• Exact Mass: 370.04513409
• Heavy Atom Count: 24
• Complexity: 469

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,2,3,3,4,4,5,5-Octafluoro-1,6-hexyldiacrylate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC(=O)OCC(C(C(C(COC(=O)C=C)(F)F)(F)F)(F)F)(F)F

Technology Process of 1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane

There total 1 articles about 1,6-Bis(acryloyloxy)-2,2,3,3,4,4,5,5-octafluorohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediol (355-74-8) + acrylic acid (79-10-7) → (2,2,3,3,4,4,5,5-octafluoro-1,6-hexadiyl)di(acrylate) (2264-01-9)

Guidance literature:

With trifluoroacetic anhydride;

DOI:10.1134/S0012500812090066

Reference yield: 89.0%

(2,2,3,3,4,4,5,5-octafluoro-1,6-hexadiyl)di(acrylate) (2264-01-9) + [(2,6-iPrC6H3NC(Me)C(Me)N-2,6-iPrC6H3)Pd(CH3)(Cl)] + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → C70H96F8N4O4Pd2(2+)*2C32H12BF24(1-)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jacs.0c10588

upstream raw materials:

2,2,3,3,4,4,5,5-octafluoro-1,6-hexanediol

acrylic acid