N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

Base Information

Chemical Name:N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide
CAS No.:500767-07-7
Molecular Formula:C₁₅H₁₉F₃N₂O₆S
Molecular Weight:412.387
Hs Code.:

Synonyms:N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

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Chemical Property of N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

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Technology Process of N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

There total 5 articles about N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 500767-06-6
N-(tert-butyloxycarbonyl)-m-L-tyrosine amide

: 500767-07-7
N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

Guidance literature:: With potassium carbonate; triethylamine; In dichloromethane; for 0.5h; Heating;
DOI:10.1021/jm020951i

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 500767-07-7
N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / aq. NaHCO₃ / tetrahydrofuran / 20 °C

2: 89 percent / K₂CO₃; Et₃N / CH₂Cl₂ / 0.5 h / Heating

With sodium hydrogencarbonate; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm020951i

Reference yield:

: 587-33-7,775-06-4,2180-37-2,32140-49-1,29562-33-2
m-tyrosine

: 500767-07-7
N-(tert-butyloxycarbonyl)-m-(trifluoromethanesulfonyloxy)-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 4 steps

1: AcCl / 20 °C

2: NH₃ / methanol / 20 °C

3: 77 percent / aq. NaHCO₃ / tetrahydrofuran / 20 °C

4: 89 percent / K₂CO₃; Et₃N / CH₂Cl₂ / 0.5 h / Heating

With ammonia; sodium hydrogencarbonate; potassium carbonate; triethylamine; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm020951i