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Technology Process of (C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

Base Information
  • Chemical Name:(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6
  • CAS No.:341489-77-8
  • Molecular Formula:C40H45FeP2Ru*F6P
  • Molecular Weight:889.626
  • Hs Code.:
(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=((C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3))PF<sub>6</sub>

Synonyms:(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

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Chemical Property of (C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6
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Technology Process of (C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

There total 1 articles about (C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

thallium(I) hexafluorophosphate
60969-19-9

thallium(I) hexafluorophosphate

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)RuH(P(C<sub>6</sub>H<sub>5</sub>)3)
341489-74-5

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)RuH(P(C6H5)3)

hydrogen
1333-74-0

hydrogen

thallium chloride
55172-29-7,7791-12-0

thallium chloride

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=((C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3))PF<sub>6</sub>
341489-77-8

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

Guidance literature:
In dichloromethane; TlPF6 was added to soln. Cp*Fe(PC4HMe2CH2C5H4)RuCl(PPh3) in CH2Cl2 and stirred for 3 h under H2 atm. at room temp.; ppt. was filtered off, ether was to filtrate;
DOI:10.1021/om0010262

Reference yield: 72.0%

pyridine
110-86-1

pyridine

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=((C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(H<sub>2</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3))PF<sub>6</sub>
341489-77-8

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(H2)(P(C6H5)3))PF6

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(NC<sub>5</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=((C<sub>5</sub>(CH<sub>3</sub>)5)Fe(PC<sub>4</sub>H(CH<sub>3</sub>)2CH<sub>2</sub>C<sub>5</sub>H<sub>4</sub>)Ru(NC<sub>5</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3))PF<sub>6</sub>
341489-80-3

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(NC5H5)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(NC5H5)(P(C6H5)3))PF6

hydrogen
1333-74-0

hydrogen

Guidance literature:
In dichloromethane; to soln. (Cp*Fe(PC4HMe2CH2C5H4)Ru(H2)(PPh3))PF6 in CH2Cl2 was added pyridine; sovent was removed, residue was chromed on silica CH2Cl2/THF 1:1; elem. nal.;
DOI:10.1021/om0010262
upstream raw materials:

thallium(I) hexafluorophosphate

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)RuH(P(C6H5)3)

hydrogen

Downstream raw materials:

(C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(NC5H5)(P(C6H5)3)(1+)*PF6(1-)=((C5(CH3)5)Fe(PC4H(CH3)2CH2C5H4)Ru(NC5H5)(P(C6H5)3))PF6

hydrogen

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