4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Base Information

Chemical Name:4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)
CAS No.:188119-62-2
Molecular Formula:C₃₂H₃₂NO₈P
Molecular Weight:589.582
Hs Code.:

Synonyms:4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Suppliers and Price of 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

There total 5 articles about 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-21-1
ethylene glycol

: 188119-59-7
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

: 188119-62-2
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Heating;
DOI:10.1021/ja9635589

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 188119-62-2
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / Br₂; AlCl₃ / tetrahydrofuran / 40 h / 0 °C

2: 89 percent / benzene / 2 h / Heating

3: 96 percent / p-toluenesulfonic acid / benzene / 24 h / Heating

With aluminium trichloride; bromine; toluene-4-sulfonic acid; In tetrahydrofuran; benzene; 1: Bromination / 2: Esterification / 3: Condensation;
DOI:10.1021/ja9635589

Reference yield:

: 99-92-3
p-aminobenzophenone

: 188119-62-2
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate (ethylene ketal)

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / NaOH / dioxane; H₂O / 2.5 h / 0 - 25 °C

2: 93 percent / Br₂; AlCl₃ / tetrahydrofuran / 40 h / 0 °C

3: 89 percent / benzene / 2 h / Heating

4: 96 percent / p-toluenesulfonic acid / benzene / 24 h / Heating

With sodium hydroxide; aluminium trichloride; bromine; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; water; benzene; 1: alkoxycarbonylation / 2: Bromination / 3: Esterification / 4: Condensation;
DOI:10.1021/ja9635589