4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

Base Information

Chemical Name:4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate
CAS No.:188119-59-7
Molecular Formula:C₃₀H₂₈NO₇P
Molecular Weight:545.529
Hs Code.:

Synonyms:4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

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Chemical Property of 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

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Technology Process of 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

There total 4 articles about 4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 53148-15-5
tetramethylammonium dibenzyl phosphate

: 157014-41-0
4-((carbobenzyloxy)amino)phenacyl bromide

: 188119-59-7
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1021/ja9635589

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 188119-59-7
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Br₂; AlCl₃ / tetrahydrofuran / 40 h / 0 °C

2: 89 percent / benzene / 2 h / Heating

With aluminium trichloride; bromine; In tetrahydrofuran; benzene; 1: Bromination / 2: Esterification;
DOI:10.1021/ja9635589

Reference yield:

: 99-92-3
p-aminobenzophenone

: 188119-59-7
4-((carbobenzyloxy)amino)phenacyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaOH / dioxane; H₂O / 2.5 h / 0 - 25 °C

2: 93 percent / Br₂; AlCl₃ / tetrahydrofuran / 40 h / 0 °C

3: 89 percent / benzene / 2 h / Heating

With sodium hydroxide; aluminium trichloride; bromine; In tetrahydrofuran; 1,4-dioxane; water; benzene; 1: alkoxycarbonylation / 2: Bromination / 3: Esterification;
DOI:10.1021/ja9635589