2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

Base Information

Chemical Name:2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene
CAS No.:558461-65-7
Molecular Formula:C₂₃H₃₁ClF₂O₃SSi
Molecular Weight:489.099
Hs Code.:

Synonyms:2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

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Technology Process of 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

There total 1 articles about 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 470716-51-9
2-[[(4-chlorophenyl)sulfonyl]methyl]-1,4-difluorobenzene

: 92511-12-1
1-{[dimethyl(1,1-dimethylethyl)silyl]oxy}-4-iodobutane

: 558461-65-7
2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

Guidance literature:: 2-[[(4-chlorophenyl)sulfonyl]methyl]-1,4-difluorobenzene; With n-butyllithium; In 1,2-dimethoxyethane; hexane; at -78 - 20 ℃; for 1.5h;

1-{[dimethyl(1,1-dimethylethyl)silyl]oxy}-4-iodobutane; In 1,2-dimethoxyethane; hexane; at -78 - 20 ℃; for 15h;

With water; In 1,2-dimethoxyethane; hexane;

Reference yield: 80.0%

: 558461-65-7
2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

: 74-88-4
methyl iodide

: 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]-1-methylpentyl]-1,4-difluorobenzene

Guidance literature:: 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h;

With water; In tetrahydrofuran; hexane;

Reference yield: 73.0%

: 558461-65-7
2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene

: 542-69-8
1-iodo-butane

: 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]-1-butylpentyl]-1,4-difluorobenzene

Guidance literature:: 2-[5-(t-Butyldimethylsilyloxy)-1-[(4-chlorophenyl)sulfonyl]pentyl]-1,4-difluorobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

1-iodo-butane; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 20h;