4--4'-nitrobenzophenone

Base Information

• Chemical Name: 4--4'-nitrobenzophenone
• CAS No.: 133041-71-1
• Molecular Formula: C₁₇H₁₈N₂O₅
• Molecular Weight: 330.34

Synonyms:4--4'-nitrobenzophenone

Chemical Property of 4--4'-nitrobenzophenone

Chemical Property:

Purity/Quality:

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Technology Process of 4--4'-nitrobenzophenone

There total 3 articles about 4--4'-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(4-fluorobenzoyl)-nitrobenzene (2195-47-3) + 2,2'-iminobis[ethanol] (111-42-2) → 4--4'-nitrobenzophenone (133041-71-1)

Guidance literature:

In dimethyl sulfoxide; for 5h; Reflux;

DOI:10.1016/j.bmc.2010.10.042

Reference yield:

fluorobenzene (462-06-6) → 4--4'-nitrobenzophenone (133041-71-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / AlCl₃ / various solvent(s) / 4 h / 20 °C

2: 60 percent / dimethylsulfoxide / 5 h / 140 °C

With aluminium trichloride; In dimethyl sulfoxide;

DOI:10.1021/jm00109a005

Reference yield:

4-nitro-benzoyl chloride (122-04-3) → 4--4'-nitrobenzophenone (133041-71-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / AlCl₃ / various solvent(s) / 4 h / 20 °C

2: 60 percent / dimethylsulfoxide / 5 h / 140 °C

With aluminium trichloride; In dimethyl sulfoxide;

DOI:10.1021/jm00109a005

upstream raw materials:

4-(4-fluorobenzoyl)-nitrobenzene

2,2'-iminobis[ethanol]

fluorobenzene

4-nitro-benzoyl chloride

Downstream raw materials:

(4-{Bis-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-amino}-phenyl)-(4-nitro-phenyl)-methanone

(4-Amino-phenyl)-{4-[bis-(2-hydroxy-ethyl)-amino]-phenyl}-methanone

C₁₇H₂₀Cl₂N₂

2-[[4-(4-Amino-benzyl)-phenyl]-(2-hydroxy-ethyl)-amino]-ethanol

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