N,N-dimethyl 2-benzoyl-2-propane selenenamide

Base Information

• Chemical Name: N,N-dimethyl 2-benzoyl-2-propane selenenamide
• CAS No.: 81360-91-0
• Molecular Formula: C₁₂H₁₇NOSe
• Molecular Weight: 270.233
• Mol file: 81360-91-0.mol

Synonyms:N,N-dimethyl 2-benzoyl-2-propane selenenamide

Chemical Property of N,N-dimethyl 2-benzoyl-2-propane selenenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-dimethyl 2-benzoyl-2-propane selenenamide

There total 9 articles about N,N-dimethyl 2-benzoyl-2-propane selenenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide (81360-89-6) + dimethyl amine (124-40-3) → 2-methyl-1-phenylprop-2-en-1-one (769-60-8) + N,N-dimethyl 2-benzoyl-2-propane selenenamide (81360-91-0) + bis-(2-benzoyl-2-propyl) diselenide (81360-90-9) + phenyl isopropyl ketone (611-70-1)

Guidance literature:

In dichloromethane; at -30 ℃; for 0.5h; Further byproducts given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(01)96716-X

Reference yield:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide (81360-89-6) → N,N-dimethyl 2-benzoyl-2-propane selenenamide (81360-91-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trimethyl phosphite

With phosphorous acid trimethyl ester;

DOI:10.1021/ja00374a047

Reference yield:

2-methyl-1-phenyl-1-trimethylsiloxy-1-propene (39158-85-5) → N,N-dimethyl 2-benzoyl-2-propane selenenamide (81360-91-0)

Guidance literature:

Multi-step reaction with 2 steps

1: SeCl₂

With selenium(II) chloride;

DOI:10.1021/ja00374a047

upstream raw materials:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide

dimethyl amine

1-phenyl-2-(chloroseleno)-2-methylpropanone

bis-(2-benzoyl-2-propyl) diselenide