4-ethoxybenzaldehyde dimethyl acetal

Base Information

• Chemical Name: 4-ethoxybenzaldehyde dimethyl acetal
• CAS No.: 82736-90-1
• Molecular Formula: C₁₁H₁₆O₃
• Molecular Weight: 196.246
• Mol file: 82736-90-1.mol

Synonyms:4-ethoxybenzaldehyde dimethyl acetal

Chemical Property of 4-ethoxybenzaldehyde dimethyl acetal

Chemical Property:

Purity/Quality:

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Technology Process of 4-ethoxybenzaldehyde dimethyl acetal

There total 4 articles about 4-ethoxybenzaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

→ 4-ethoxybenzaldehyde dimethyl acetal (82736-90-1)

Guidance literature:

With copper(II) tetrafluoroborate monohydrate; In methanol; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 81.0%

4-ethoxybenzaldehyde (10031-82-0) + trimethyl orthoformate (149-73-5) → 4-ethoxybenzaldehyde dimethyl acetal (82736-90-1)

Guidance literature:

With hydrogenchloride; water; In methanol; at 20 ℃; for 48h;

DOI:10.1016/j.carres.2012.03.021

Reference yield: 50.0%

methanol (67-56-1) + 4,4'-diethoxybenzalazine (99163-21-0) → 4-ethoxybenzaldehyde dimethyl acetal (82736-90-1)

Guidance literature:

With [bis(acetoxy)iodo]benzene; sodium methylate; at 0 - 25 ℃; for 48h;

DOI:10.1016/S0040-4039(00)87152-X

upstream raw materials:

methanol

4,4'-diethoxybenzalazine

4-ethoxybenzaldehyde

trimethyl orthoformate

Downstream raw materials:

C₁₆H₂₂O₇