1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole
CAS No.:1448005-23-9
Molecular Formula:C₂₉H₂₇N₉O
Molecular Weight:517.593
Hs Code.:

Synonyms:1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

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Chemical Property of 1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

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Technology Process of 1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

There total 8 articles about 1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1191952-85-8
tris(1-benzyl-1H-1,2,3-triazol-4-yl)methanol

: 74-88-4
methyl iodide

: 1448005-23-9
1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: tris(1-benzyl-1H-1,2,3-triazol-4-yl)methanol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 23 ℃; for 2h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 - 23 ℃; for 14h; Inert atmosphere;
DOI:10.1002/adsc.201300887

Reference yield:

: 67-56-1
methanol

: C₂₈H₂₄N₉⁽¹⁺⁾*C₂F₃O₂^(1-)

: 1448005-23-9
1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.05.138

Reference yield:

: 100-39-0
benzyl bromide

: 1448005-23-9
1-benzyl-4-(bis(1-benzyl-1H-1,2,3-triazol-4-yl)(methoxy)methyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / acetone; water / 24 h / 20 °C / Inert atmosphere

2: copper(II) sulfate; sodium L-ascorbate / water; ethanol / 12 h / 20 °C / Inert atmosphere

3: dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4: dichloromethane / 3 h / 0 °C / Inert atmosphere

With sodium azide; copper(II) sulfate; sodium L-ascorbate; In ethanol; dichloromethane; water; acetone; 2: |Huisgen Cycloaddition;
DOI:10.1016/j.tetlet.2013.05.138