methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

Base Information

Chemical Name:methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate
CAS No.:885129-57-7
Molecular Formula:C₂₆H₂₈O₄
Molecular Weight:404.506
Hs Code.:

Synonyms:methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

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Chemical Property of methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

Chemical Property:

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Technology Process of methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

There total 5 articles about methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885129-56-6
4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoic acid

: 74-88-4
methyl iodide

: 885129-57-7
methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

Guidance literature:: 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoic acid; methyl iodide; With caesium carbonate; In N,N-dimethyl-formamide; for 2h;

With water; ammonium chloride; In N,N-dimethyl-formamide;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 885129-57-7
methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0 °C

2.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 1 h / 50 °C

2.2: 20 °C

2.3: 0.5 h

3.1: iodine; magnesium; lithium chloride / tetrahydrofuran / 50 °C

3.2: 0 - 20 °C

4.1: sodium carbonate / N,N-dimethyl-formamide

With lithium hydroxide monohydrate; water; iodine; sodium carbonate; magnesium; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 131379-16-3
4-(ethoxycarbonyl)phenylzinc iodide

: 885129-57-7
methyl 4-{1-[4-(benzyloxy)phenyl]-1-hydroxy-2,2-dimethylpropyl} benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0 °C

2.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 1 h / 50 °C

2.2: 20 °C

2.3: 0.5 h

3.1: iodine; magnesium; lithium chloride / tetrahydrofuran / 50 °C

3.2: 0 - 20 °C

4.1: sodium carbonate / N,N-dimethyl-formamide

With lithium hydroxide monohydrate; water; iodine; sodium carbonate; magnesium; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;