C₁₂H₁₈ClOP

Base Information

Chemical Name:C₁₂H₁₈ClOP
CAS No.:344332-09-8
Molecular Formula:C₁₂H₁₈ClOP
Molecular Weight:244.701
Hs Code.:

Synonyms:C₁₂H₁₈ClOP

Suppliers and Price of C₁₂H₁₈ClOP

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₈ClOP

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of C₁₂H₁₈ClOP

There total 1 articles about C₁₂H₁₈ClOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-57-8
2-monochlorophenol

: 40244-90-4
Chlorodiisopropylphosphane

: 344332-09-8
C₁₂H₁₈ClOP

Guidance literature:: With triethylamine; In toluene; for 15h; Reflux; Inert atmosphere;
DOI:10.1021/ol303203m

Reference yield:

: 344332-09-8
C₁₂H₁₈ClOP

: 85-97-2
2-chloro-6-phenylphenol

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylsulfide borane complex / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: toluene / 1 h / 20 °C / Schlenk technique; Inert atmosphere

3: toluene; fluorobenzene / 16 h / 140 °C / Inert atmosphere

4: potassium hydrogen difluoride / toluene; methanol; water / 2 h / 0 - 20 °C / Schlenk technique; Sealed tube; Cooling; Inert atmosphere

5: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 80 °C / Inert atmosphere; Sonication; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium hydrogen difluoride; dimethylsulfide borane complex; potassium carbonate; In methanol; fluorobenzene; ethanol; dichloromethane; water; toluene; 5: |Suzuki Coupling;
DOI:10.1021/ol303203m